NMR Equipment

 

The NMR lab at ENS hosts

  1. 800 MHz/527 GHz MAS-DNP system with Avance III
    • Solid Probes
      • 3.2 mm MAS-DNP HXY probe (100 K), 32 ul/15 kHz-sapphire or 46 ul thin-walled Zr
      • 3.2 mm MAS E-free (1H, 13C, 15N), 30 ul/24 kHz, -30° to +70°
      • 2.5 mm MAS HXY probe-double (X: 31P-15N) or triple (X/Y: 31P-11B/23Na-2H), 12ul/35 kHz
      • 1.3 mm MAS (1H, 13C, 15N), 2.5ul/67 kHz, -30° to +70°
    • Liquid Probes
      • TXI (1H / 13C,15N,2H), 5mm, triple gradients, ATM, -50 to +80°C
      • BBO (X /1H,19F,2H), 5 mm, z gradient, X: 31P-107Ag, ATM, -150 to +150°C
    • Imaging Probes
      • résonateur 25mm 1H (bird-cage)
      • résonateur 20mm 1H/13C (saddle-coil)
      •  résonateur 10mm 1H/13C (saddle-coil)
      •  résonateur 5mm 1H/13C (saddle-coil)
  2. 600 MHz solution-state NMR system with Avance III
    • TXI (1H, 13C, 15N), 5mm, gradients xyz
    • TBI (1H, 13C, X), 5 mm, gradients xyz
    • TXO (1H, 13C, 15N), 3.2 mm, z gradient (Shuttle)
    • 2F-NMR operating between 14.1 T and 0.33 T, z gradient at high field and low field
    • Cryoprobe
  3. 500 MHz solution-state NMR system (Installed by 2021)
  4. 400 MHz solid-state NMR system with Avance III (solid/liquid)
    • Liquid Probes
      • TXI (1H, 13C, 15N), 5 mm, gradient-z
      • TXI (1H, 13C, 15N), 10 mm
    • Solid Probes
      • MAS (1H, X, Y) 1.3 mm
      • MAS (1H, X, Y) 2.5 mm
      • MAS (1H, X, Y) 4 mm
      • MAS (1H, 13C/31P) 4 mm
      • MAS (1H, X, Y) 7 mm
  5. 6.7 T/188 GHz Dissolution DNP Polarizer
  6. 9.4 T/263 GHz Dissolution DNP Polarizer
  7. 9.4 T/263 GHz Dissolution DNP Polarizer (Installed by 2021)